Ammonium nitrate (even technical grade) is melted
in a melter. The molten ammonium nitrate flows into
a combustion pot where ammonium nitrate is decomposed
according to the following reaction:
NH4NO3 ------------ N2O + 2H2O
The reaction is ticklish and has to be controlled properly.
If temperature of ammonium nitrate is allowed to go
beyond a certain point then we do not yet yield. In
our plant we almost get yield of reaction equal to 95%
or even more. In practice, however, with N2O some other
impurities are also obtained as products of combustion.
There is some undecomposed ammonium nitrate, with its
fumes. These are recovery in the primary scrubber. The
steam in the hot gas is condensed in the first water
scrubber and the entrained moisture and traces of ammonium
nitrate get separated in the mist separator. The residual
traces of ammonium nitrate, carbon dioxide and other
oxides of nitrogen are removed in the caustic scrubber.
Nitrous oxide as an oxide gas for atomic absorption
in spectrophotometer and as fuel oxidant for racing
vehicles.
The gas containing some nitrogen is then stored in the
gas balloon. The gas is compressed with a compressor,
dried in a drier and then refrigerate when it becomes
liquid. Liquid nitrous oxide is stored in high-pressure
storage vessel into cylinders and the gas is filled
by weight. In a low pressure plant the gas after refrigeration
is stored in a storage tank and from there it is filled
in cylinders with a pump. Each batch is analyzed in
the laboratory to ensure quality of the product and
proper record is maintained.
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